4-(己氧基)苯基-4-(癸基氧基)苯甲酸盐合成路线 (共 6 条)
反应条件
1: K2CO3 / cyclohexanone / 12 h / Heating
2: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: K2CO3 / acetone / 6 h / Heating
2: aq. KOH / methanol / 12 h / Heating
3: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: aq. KOH / methanol / 12 h / Heating
2: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: K2CO3 / acetone / 6 h / Heating
2: aq. KOH / methanol / 12 h / Heating
3: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
1: K2CO3 / cyclohexanone / 12 h / Heating
2: DCC, DMAP / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane
3 h; Ambient temperature; Yield given;
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44