反应条件
1.1: 4.00 g / N-iodosuccinimide; AgNO3 / acetone / 3.5 h / 0 °C
2.1: BH3*SMe2; cyclohexene / diethyl ether / 1 h / 0 °C
2.2: 82 percent / glacial AcOH / diethyl ether / 0.5 h / 0 °C
3.1: (1S)-(+)-10-camphorsulfonic acid / methanol / 2 h / 0 °C
3.2: 75 percent / MnO2 / CH2Cl2 / 14 h / 20 °C
View Scheme
参考文献
Tanaka, Hiroshi; Hasegawa, Tsuyoshi; Iwashima, Makoto; Iguchi, Kazuo; Takahashi, Takashi
Organic Letters, 2004 , vol. 6, # 7 p. 1103 - 1106
