反应条件
1: 52 percent / LAH / diethyl ether / 1a) overnight, 1b) reflux, 6 h
2: 74 percent / PBr3, pyridine / diethyl ether / 1a) overnight, 2) reflux, 2 h
3: 1) sodium / 1) benzene, DMF, 2) benzene, reflux, 12 h
4: 58 percent / NaCl / H2O; dimethylsulfoxide / 8 h / 180 °C
View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Kumari, Sarla; Rani, Veena
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 675 - 676
