2-氯-7-甲氧基喹啉-3-甲醛合成路线 （共 9 条）
反应条件
trichlorophosphate 4 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1520 - 1530
反应条件
1: H2O 2: 89 percent / POCl3 / 80 - 90 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 45, # 1 p. 292 - 296
反应条件
trichlorophosphate Heating;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 9 p. 1868 - 1875
反应条件
ammonia; iodine in tetrahydrofuran; water T=20°C; 1.41667 h;
参考文献
Upadhyay, Shraddha; Chandra, Atish; Singh, Radhey M.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 1 p. 152 - 154
反应条件
acetic acid in water Heating;
参考文献
Srivastava, Ambika; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 9 p. 1868 - 1875
反应条件
sodium tetrahydroborate in methanol T=20°C;
参考文献
Pokalwar; Hangarge; Kategaonkar; Shingare
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 3 p. 430 - 433
反应条件
bromine in various solvent(s) T=120 - 130°C; 0.5 h;
参考文献
Cziaky
Synthetic Communications, 1991 , vol. 21, # 18-19 p. 1929 - 1934
反应条件
formic acid; triethylamine; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=110°C;
参考文献
Sato, Itaru; Nakao, Tomohiko; Sugie, Rie; Kawasaki, Tsuneomi; Soai, Kenso
Synthesis, 2004 , # 9 p. 1419 - 1428
反应条件
1: 30 percent / H2 / catalytic hydrogenation
2: 1.) sodium methylate / 1.) DMSO, 30 min, 75 deg C, 2.) 75 deg C, 5-10 min
3: 80 percent / propan-2-ol / 0.17 h / Heating
4: 35 percent / sodium methylate / ethanol / 40 h / Heating
View Scheme
参考文献
Gatti; Cavrini; Roveri; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 5 p. 468 - 474
