2-氯-7-甲基-3-喹啉甲醛合成路线 （共 13 条）
反应条件
trichlorophosphate T=80 - 90°C; Vilsmeier-Haack cyclisation; 6 h;
参考文献
Srivastava, Ambika; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 9 p. 1868 - 1875
反应条件
sodium hydroxide; zinc in ethanol 120 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2509 - 2517
反应条件
1.1: triethylamine / chloroform / 1 h / 0 °C 2.1: trichlorophosphate / 0 - 75 °C / Inert atmosphere 2.2: 0.5 h / 0 - 10 °C / Inert atmosphere View Scheme
参考文献
Heterocyclic Communications, , vol. 17, # 3-4 p. 111 - 119
反应条件
1: 87 percent / toluene-p-sulphonic acid / benzene / Heating 2: 87 percent / BuLi, H2O / diethyl ether; hexane / -70 °C 3: 0.08 g / aq. HCl / diethyl ether; hexane View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2509 - 2517
反应条件
1: 87 percent / BuLi, H2O / diethyl ether; hexane / -70 °C 2: 0.08 g / aq. HCl / diethyl ether; hexane View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2509 - 2517
反应条件
hydrogenchloride in diethyl ether 1 h; Ambient temperature; Yield given;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
反应条件
trichlorophosphate Heating;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 9 p. 1868 - 1875
参考文献
Chemical Papers, , vol. 64, # 6 p. 812 - 817
反应条件
hydrogenchloride; n-butyllithium 1.) ether, hexane, -70 deg C, 2.) ether , 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2509 - 2517
反应条件
trichlorophosphate Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1531 - 1536
