2-氯-6,7-二甲氧基-3-喹啉甲醛合成路线 (共 6 条)
反应条件
hydrogenchloride 1 h; Heating;
参考文献
Tilakraj, T.; Ambekar, Sarvottam Y.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 3 p. 251 - 253
反应条件
dicyclohexyl-carbodiimide; pyridinium chlorochromate in chloroform
T=30°C; 0.5 h;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1286 - 1287
反应条件
trichlorophosphate
2 h; Heating;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1520 - 1530
反应条件
1.1: triethylamine / chloroform / 1 h / 0 °C
2.1: trichlorophosphate / 0 - 75 °C / Inert atmosphere
2.2: 0.5 h / 0 - 10 °C / Inert atmosphere
View Scheme
参考文献
Srihari, Ejjirothu; Kumar, Gangala Siva; Kumar, Chebolu Naga Sesha Sai Pavan; Seth, Ratnesh Kumar; Biswas, Sukla; Sridhar, Balasubramanian; Rao, Vaidya Jayathirtha
Heterocyclic Communications, 2011 , vol. 17, # 3-4 p. 111 - 119
反应条件
sodium tetrahydroborate in methanol
参考文献
Bhat, Balkrishen; Bhaduri, A. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 33 - 37
反应条件
hydrogen
catalytic hydrogenation;
参考文献
Gatti; Cavrini; Roveri; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 5 p. 468 - 474