cesium fluoride
T=200°C; 16 h; Title compound not separated from byproducts;
参考文献
Bryce, Martin R.; Chambers, Richard D.; Kirk, Julian R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1391 - 1395
1: 62 percent / sodium hypochlorite / acetonitrile; H2O / 40 h / Ambient temperature
2: caesium fluoride / 16 h / 200 °C
View Scheme
参考文献
Bryce, Martin R.; Chambers, Richard D.; Kirk, Julian R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1391 - 1395
pyridine
30 h; Ambient temperaturefurther reagent; Further byproducts given. Yields of byproduct given;
参考文献
Chambers, Richard D.; Taylor, Graham; Powell, Richard L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 429 - 434
cesium fluoride in N,N-dimethyl-formamide
24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Chambers, Richard D.; Taylor, Graham; Powell, Richard L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 426 - 428
cesium fluoride in N,N-dimethyl-formamide
240 h; Ambient temperature; Yield given;
参考文献
Chambers, Richard D.; Taylor, Graham; Powell, Richard L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 429 - 434
cesium fluoride in N,N-dimethyl-formamide
72 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Chambers, Richard D.; Taylor, Graham; Powell, Richard L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 426 - 428
pyridine
130 h; Yield given. Yields of byproduct given;
参考文献
Chambers, Richard D.; Taylor, Graham; Powell, Richard L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 426 - 428
1: caesium fluoride / dimethylformamide / 100 h / Ambient temperature
2: caesium fluoride / dimethylformamide / 24 h / Ambient temperature
View Scheme
参考文献
Chambers, Richard D.; Taylor, Graham; Powell, Richard L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 426 - 428
potassium carbonate in acetonitrile
24 h; Ambient temperature;
参考文献
Bayliff, Andrew E.; Bryce, Martin R.; Chambers, Richard D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 763 - 768
