1,2-二氢-环丁并[b]萘合成路线 （共 8 条）
反应条件
lithium aluminium tetrahydride in 1,4-dioxane
T=101°C; 5 h;
参考文献
Kitagaki, Shinji; Okumura, Yuki; Mukai, Chisato
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1849 - 1852
反应条件
copper; ammonium chloride; zinc in methanol
2 h; Heating;
参考文献
Saracoglu, Nurullah; Durucasu, Inci; Balci, Metin
Tetrahedron, 1995 , vol. 51, # 40 p. 10979 - 10986
反应条件
lithium aluminium tetrahydride in 1,4-dioxane
T=101°C; 7 h;
参考文献
Kitagaki, Shinji; Okumura, Yuki; Mukai, Chisato
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1849 - 1852
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
T=25°C;
参考文献
Angus, Richard O.; Johnson, Richard P.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 273 - 276
反应条件
T=780°C; P=0.01 Torr; 1 h;
参考文献
Abou-Teim, Omar; Goodland, Michael C.; McOmie, F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2659 - 2662
反应条件
1: 81 percent / Et3N / tetrahydrofuran / 4 h / -78 - 20 °C
2: 41 percent / LiAlH4 / dioxane / 7 h / 101 °C
View Scheme
参考文献
Kitagaki, Shinji; Okumura, Yuki; Mukai, Chisato
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1849 - 1852
反应条件
1: 77 percent / sulphuryl chloride, benzoyl chloride / CCl4 / 6 h / Heating; Irradiation
2: 30 percent / 1 h / 780 °C / 0.01 Torr
View Scheme
参考文献
Abou-Teim, Omar; Goodland, Michael C.; McOmie, F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2659 - 2662
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Thummel,R.P. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 12 p. 2473 - 2477
