tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,2-diaminocyclohexane-N,N'-bis(2'-diphenylphosphinobenzoyl); Tetrahexylammonium bromide in dichloromethane; water
T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Trost, Barry M.; Krische, Michael J.; Radinov, Rumen; Zanoni, Giuseppe
Journal of the American Chemical Society, 1996 , vol. 118, # 26 p. 6297 - 6298
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=25°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Hirata, Takaki; Sasada, Yoshihiro; Ohtani, Takashi; Asada, Takahiro; Kinoshita, Hideki; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 1 p. 75 - 96
Hirata, Takaki; Sasada, Yoshihiro; Ohtani, Takashi; Asada, Takahiro; Kinoshita, Hideki; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 1 p. 75 - 96
1: 100 percent / H2, quinoline, sodium acetate / 5percent Pd/C / methanol
2: DBU / acetonitrile / 3 h / 25 °C / other vinylic sulfones; other bases; var. temp. and time
View Scheme
参考文献
Hirata, Takaki; Sasada, Yoshihiro; Ohtani, Takashi; Asada, Takahiro; Kinoshita, Hideki; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 1 p. 75 - 96
