1: 0.33 h / 250 °C
2: 40percent peracetic acid / acetic acid / 72 h / 15 - 25 °C
3: 0.17 h / 110 °C
4: 50 percent / Jones reagent / acetone / 18 h / 25 °C
5: 92 percent / 96.6percent H2SO4 / 2 h / Heating
6: H2 / 5percent Pd/C
View Scheme
参考文献
Hoffman, William F.; Woltersdorf, Otto W.; Novello, Frederick C.; Cragoe, Edward J; Spinger, James P.; et al.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 7 p. 865 - 873
1: 0.17 h / 245 - 250 °C
2: m-chloroperbenzoic acid / CH2Cl2 / 24 h / 10 - 20 °C
View Scheme
参考文献
Hoffman, William F.; Woltersdorf, Otto W.; Novello, Frederick C.; Cragoe, Edward J; Spinger, James P.; et al.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 7 p. 865 - 873
