N-(1,3-苯并二氧戊环-5-基甲基)丙-2-胺合成路线 （共 4 条）
反应条件
[(C5Me5)IrI2]2 in anhydrous xylene
T=155°C; 10 h; Inert atmosphere;
参考文献
Saidi, Ourida; Williams, Jonathan M. J.; Blacker, A. John; Farah, Mohamed M.; Marsden, Stephen P.
Angewandte Chemie, International Edition, 2009 , vol. 48, # 40 p. 7375 - 7378
Angewandte Chemie, 2009 , vol. 121, # 40 p. 7511 - 7514
反应条件
sodium tetrahydroborate in methanol
T=20°C; 1 h;
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Nakamura, Takatoshi; Horibata, Akiyoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Yamazaki, Tetsuro; Tokuda, Masao
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5951 - 5958
反应条件
1: Na2SO4 / CH2Cl2 / 2 h
2: NaBH4 / methanol / 1 h / 20 °C
View Scheme
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Nakamura, Takatoshi; Horibata, Akiyoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Yamazaki, Tetsuro; Tokuda, Masao
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 5951 - 5958
反应条件
anschliessend hydrieren an Palladium/Kohle in Aethanol;
参考文献
Surrey; Rukwid
Journal of the American Chemical Society, 1955 , vol. 77, p. 3798,3800
