(R/S)-N-去乙酰基秋水仙裂碱合成路线 （共 6 条）
反应条件
Multi-step reaction with 4 steps 1: 79 percent / Na2CO3 / diethyl ether / 2.5 h / Ambient temperature2: 38 percent / methanol; diethyl ether / 3 h3: 70 percent / K2CO3 / acetone; H2O / 60 °C
参考文献
Dumont; Brossi; Silverton Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2515 - 2521
反应条件
Multi-step reaction with 5 steps 1: 79 percent / Na2CO3 / diethyl ether / 2.5 h / Ambient temperature2: 38 percent / methanol; diethyl ether / 3 h3: 70 percent / K2CO3 / acetone; H2O / 60 °C5: 71 percent / NaHCO3 / CHCl3; H2O / 2.5 h
参考文献
Dumont; Brossi; Silverton Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2515 - 2521
反应条件
Multi-step reaction with 2 steps 1: 79 percent / Na2CO3 / diethyl ether / 2.5 h / Ambient temperature2: 46 percent / methanol; diethyl ether / 3 h
参考文献
Dumont; Brossi; Silverton Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2515 - 2521
反应条件
Multi-step reaction with 3 steps 1: 79 percent / Na2CO3 / diethyl ether / 2.5 h / Ambient temperature2: 46 percent / methanol; diethyl ether / 3 h3: 70 percent / K2CO3 / acetone; H2O / 60 °C
参考文献
Dumont; Brossi; Silverton Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2515 - 2521
反应条件
Multi-step reaction with 2 steps 1: 79 percent / Na2CO3 / diethyl ether / 2.5 h / Ambient temperature2: 38 percent / methanol; diethyl ether / 3 h
参考文献
Dumont; Brossi; Silverton Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2515 - 2521
反应条件
Multi-step reaction with 3 steps 1: 79 percent / Na2CO3 / diethyl ether / 2.5 h / Ambient temperature2: 38 percent / methanol; diethyl ether / 3 h3: 70 percent / K2CO3 / acetone; H2O / 60 °C
参考文献
Dumont; Brossi; Silverton Journal of Organic Chemistry, 1986 , vol. 51, # 13 p. 2515 - 2521
