8-(2,2-二乙氧基乙氧基)-2,6-二甲基辛-2-烯合成路线 (共 3 条)
反应条件
1: 3,7-dimethyl-oct-6-en-1-ol With tetra-(n-butyl)ammonium iodide; sodium hydride in N,N-dimethyl-formamide; mineral oil
T=20°C; 0.5 h; Inert atmosphere;
2: 2-bromoacetaldehyde diethyl acetal in N,N-dimethyl-formamide; mineral oil
T=0 - 40°C; Inert atmosphere;
参考文献
Li, Jingwei; Sun, Chunrui; Lee, Daesung
Journal of the American Chemical Society, 2010 , vol. 132, # 19 p. 6640 - 6641
参考文献
Houbigant; Sabetay
Patent: FR37584 ;
Full Text Show Details
Sabetay
Bulletin de la Societe Chimique de France, 1929 , vol. <4> 45, p. 1167
反应条件
sulfuric acid; acetic acid
参考文献
Li, Jingwei; Sun, Chunrui; Lee, Daesung
Journal of the American Chemical Society, 2010 , vol. 132, # 19 p. 6640 - 6641