反应条件
in ethylene glycol dimethyl ether; isopropyl alcohol
byproducts: NaCl; absence of moisture; dropwise addn. of BuSnCl3 to 3 equiv. of alkoxide (in i-PrOH/DME=1:2 v/v), refluxing for 3 h; filtration off of NaCl, evapn. (reduced pressure), distn. (vac.);
参考文献
Banse, Frederic; Ribot, F.; Toledano, P.; Maquet, J.; Sanchez, C.
Inorganic Chemistry, 1995 , vol. 34, p. 6371 - 6379
