5-甲基-1-苯基-1H-吡唑合成路线 (共 30 条)
反应条件
hydroxybenzaldoxime; copper(I) oxide in acetonitrile T=82°C; 24 h;
参考文献
European Journal of Organic Chemistry, , # 4 p. 695 - 709
反应条件
nickel in ethanol Heating;
参考文献
Peruncheralathan; Khan; Ila; Junjappa
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 10030 - 10035
反应条件
ethylene glycol; toluene-4-sulfonic acid in benzene 48 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 49, # 15 p. 2663 - 2669
反应条件
hydroxybenzaldoxime; copper(I) oxide in acetonitrile T=82°C; 24 h;
参考文献
European Journal of Organic Chemistry, , # 4 p. 695 - 709
反应条件
toluene-4-sulfonic acid in benzene 48 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 49, # 15 p. 2663 - 2669
参考文献
Menozzi; Mosti; Schenone
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 6 p. 1669 - 1675
反应条件
n-butyllithium 1.) THF, pentane, -78 deg C, 1 h, 2.) THF, pentane, from -78 deg C to RT; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 115, # 17 p. 7645 - 7652
反应条件
1: 45 percent / ethanol / Heating 2: 85 percent / Raney Nickel / ethanol / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 24 p. 10030 - 10035
反应条件
phosphorus; phosphorus tribromide T=220°C; im Rohr; Erwaermen des Reaktionsprodukts mit Zinn und Salzsaeure;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 352, p. 328 Anm. 11
Chemische Berichte, , vol. 40, p. 484
反应条件
1: 92 percent / KOH / ethanol / 5 h / Heating 2: 98 percent / 36 h / 200 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 6 p. 1669 - 1675