2,6-二(氨基甲基)苯酚合成路线 （共 6 条）
反应条件
hydrazine hydrate in methanol
2.5 h; Heating;
参考文献
Malachowski, Mitchell R.; Davidson, Marilyn G.; Davis, J. Daniel
Heterocycles, 1992 , vol. 34, # 6 p. 1227 - 1230
反应条件
1: 61 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 6 h / Heating
2: 41 percent / dimethylformamide / 48 h / 50 °C
3: 41 percent / aq. HI / 5 h / Heating
4: H2NNH2*H2O / methanol / 2.5 h / Heating
View Scheme
参考文献
Malachowski, Mitchell R.; Davidson, Marilyn G.; Davis, J. Daniel
Heterocycles, 1992 , vol. 34, # 6 p. 1227 - 1230
反应条件
1: 41 percent / dimethylformamide / 48 h / 50 °C
2: 41 percent / aq. HI / 5 h / Heating
3: H2NNH2*H2O / methanol / 2.5 h / Heating
View Scheme
参考文献
Malachowski, Mitchell R.; Davidson, Marilyn G.; Davis, J. Daniel
Heterocycles, 1992 , vol. 34, # 6 p. 1227 - 1230
反应条件
1: 41 percent / aq. HI / 5 h / Heating
2: H2NNH2*H2O / methanol / 2.5 h / Heating
View Scheme
参考文献
Malachowski, Mitchell R.; Davidson, Marilyn G.; Davis, J. Daniel
Heterocycles, 1992 , vol. 34, # 6 p. 1227 - 1230
反应条件
1: 69 percent / NBS, AIBN / methyl formate / 3 h / Heating; Irradiation
2: dimethylformamide / 3 h / 80 °C
3: 3 M aq. HCl / 7 h / Heating
View Scheme
参考文献
Muche, Marc-Steffen; Goebel, Michael W.
Angewandte Chemie, 1996 , vol. 108, # 18 p. 2263 - 2265
反应条件
1: dimethylformamide / 3 h / 80 °C
2: 3 M aq. HCl / 7 h / Heating
View Scheme
参考文献
Muche, Marc-Steffen; Goebel, Michael W.
Angewandte Chemie, 1996 , vol. 108, # 18 p. 2263 - 2265
