(9ci)-4,4-二乙基-3,4-二氢-1H-2-苯并吡喃-1-酮合成路线 （共 3 条）
反应条件
1: DIPEA / CH2Cl2 / 20 °C
2: TiCl4 / CH2Cl2 / 0 °C
3: KMnO4; CuSO4*5H2O / CH2Cl2 / 20 °C
View Scheme
参考文献
Nagao, Yoshimitsu; Tanaka, Satoru; Hayashi, Kazuhiko; Sano, Shigeki; Shiro, Motoo
Synlett, 2004 , # 3 p. 481 - 484
反应条件
1: LiAlH4 / tetrahydrofuran / Heating
2: DIPEA / CH2Cl2 / 20 °C
3: TiCl4 / CH2Cl2 / 0 °C
4: KMnO4; CuSO4*5H2O / CH2Cl2 / 20 °C
View Scheme
参考文献
Nagao, Yoshimitsu; Tanaka, Satoru; Hayashi, Kazuhiko; Sano, Shigeki; Shiro, Motoo
Synlett, 2004 , # 3 p. 481 - 484
反应条件
1: NaH / tetrahydrofuran / 20 °C
2: LiAlH4 / tetrahydrofuran / Heating
3: DIPEA / CH2Cl2 / 20 °C
4: TiCl4 / CH2Cl2 / 0 °C
5: KMnO4; CuSO4*5H2O / CH2Cl2 / 20 °C
View Scheme
参考文献
Nagao, Yoshimitsu; Tanaka, Satoru; Hayashi, Kazuhiko; Sano, Shigeki; Shiro, Motoo
Synlett, 2004 , # 3 p. 481 - 484
