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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6833-19-8
合成路线
（共 47 条）
24973-91-9
→
反应条件
6833-19-8
反应条件
1: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 4.5 h / Heating 2: 83 percent Turnov. / sodium methoxide / ethanol / 48 h / Heating 3: 93 percent / N-chlorosuccinimide / CCl4 / 12 h / Heating 4: 12 percent / aq sodium carbonate / 48 h / 20 - 25 °C / further reagents 5: 81 percent / benzene / 4 h / 65 °C View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85924-73-8
→
反应条件
6833-19-8
反应条件
1: 25 mg / tetrahydrofuran / 0.17 h / -78 °C 2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 4.5 h / Heating 3: 83 percent Turnov. / sodium methoxide / ethanol / 48 h / Heating 4: 93 percent / N-chlorosuccinimide / CCl4 / 12 h / Heating 5: 12 percent / aq sodium carbonate / 48 h / 20 - 25 °C / further reagents 6: 81 percent / benzene / 4 h / 65 °C View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85864-98-8
→
反应条件
6833-19-8
反应条件
1: 15 percent / tetrahydrofuran / 48 h / Heating 2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 4.5 h / Heating 3: 83 percent Turnov. / sodium methoxide / ethanol / 48 h / Heating 4: 93 percent / N-chlorosuccinimide / CCl4 / 12 h / Heating 5: 12 percent / aq sodium carbonate / 48 h / 20 - 25 °C / further reagents 6: 81 percent / benzene / 4 h / 65 °C View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
4780-79-4
1-萘甲醇
+
74497-02-2
→
反应条件
6833-19-8
反应条件
oxygen; lithium hydroxide hydrate in water T=50°C; 12 h;
参考文献
Wang, Ye; Zhu, Dapeng; Tang, Lin; Wang, Sujing; Wang, Zhiyong
Angewandte Chemie - International Edition, 2011 , vol. 50, # 38 p. 8917 - 8921
85924-90-9
→
反应条件
6833-19-8
反应条件
1: 93 percent / N-chlorosuccinimide / CCl4 / 12 h / Heating 2: 12 percent / aq sodium carbonate / 48 h / 20 - 25 °C / further reagents 3: 81 percent / benzene / 4 h / 65 °C View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85925-09-3
→
反应条件
6833-19-8
反应条件
1: 12 percent / aq sodium carbonate / 48 h / 20 - 25 °C / further reagents 2: 81 percent / benzene / 4 h / 65 °C View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
85924-89-6
→
反应条件
6833-19-8
反应条件
1: tert-butyllithium / 1.) THF, pentane, room temperature, 2.) 1 h 2: 1.) ozone, 2.) dimethyl sulfide / 1.) ethyl acetate, -78 deg C, 2.) room temperature, 5 h 3: 81 percent / benzene / 4 h / 65 °C View Scheme
参考文献
Card,P.J.; Friedli,F.E.; Shechter,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 6104
201230-82-2
+
90-11-9
1-溴代萘
+
74497-02-2
→
反应条件
6833-19-8
反应条件
tributyl-amine; palladium dichloride T=130°C; P=760 Torr; 25 h;
参考文献
Cai, Ming-Zhong; Song, Cai-Sheng; Huang, Xian
Synthetic Communications, 1997 , vol. 27, # 3 p. 361 - 366
13922-41-3
1-萘硼酸
+
103-71-9
异氰酸苯酯
→
反应条件
604-53-5
1,1'-联萘
+
6833-19-8
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran T=20°C; 40 h; Inert atmosphere;
参考文献
Kianmehr, Ebrahim; Rajabi, Azam; Ghanbari, Mohammad
Tetrahedron Letters, 2009 , vol. 50, # 15 p. 1687 - 1688
86-55-5
1-萘甲酸
+
74497-02-2
→
反应条件
6833-19-8
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in nitromethane 0.5 h; MillingGreen chemistry;
参考文献
Strukil, Vjekoslav; Bartolec, Boris; Portada, Tomislav; Dilovic, Ivica; Halasz, Ivan; Margetic, Davor
Chemical Communications, 2012 , vol. 48, # 99 p. 12100 - 12102
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