[1-环己烯-1,2-二基二(氧基)]二(三甲基硅烷)合成路线 （共 16 条）
反应条件
pyrrolidine in methanol 20 h; Ambient temperature;
参考文献
Matsuo, Kazumasa; Shindo, Mitsuru
Organic Letters, 2010 , vol. 12, # 22 p. 5346 - 5349
反应条件
1: 50 percent / 3 h / Heating 2: 63 percent / chloranil / xylene / 24 h / Heating View Scheme
参考文献
Matlin, Stephen A.; Barron, Kenneth
Journal of Chemical Research, Miniprint, 1990 , # 8 p. 1920 - 1943
参考文献
Matlin, Stephen A.; Barron, Kenneth
Journal of Chemical Research, Miniprint, 1990 , # 8 p. 1920 - 1943
反应条件
oxygen O2, singlet; TPP 2. Florisil in tetrachloromethane T=-20°C; 0.05 h; Irradiation; Product distribution;
参考文献
Adam, Waldemar; Wang, Xiaoheng
Tetrahedron Letters, 1990 , vol. 31, # 9 p. 1245 - 1248
反应条件
methanol; biphenyl; naphthalenyl-1-carbonitrile in acetonitrile Ambient temperatureIrradiationvar. temp., no irradiation; 1-(trimethylsiloxy)cyclohexene; Product distributionMechanism;
参考文献
Gassman, Paul G.; Bottorff, Kyle J.
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1097 - 1100
反应条件
1: Et2Zn / toluene / 2.25 h / Ambient temperature 2: FeCl3 / dimethylformamide / 3.25 h / 60 - 70 °C View Scheme
参考文献
Matzeit; Schafer; Amatore
Synthesis, 1995 , # 11 p. 1432 - 1444
反应条件
oxygen O2, singlet; TPP 2. Florisil in tetrachloromethane T=-20°C; 0.05 h; Irradiation; Product distribution;
参考文献
Tetrahedron Letters, , vol. 31, # 9 p. 1245 - 1248
反应条件
oxygen O2, singlet; TPP 2. Florisil in tetrachloromethane
T=-20°C; 0.05 h; Irradiation; Product distribution;
参考文献
Adam, Waldemar; Wang, Xiaoheng
Tetrahedron Letters, 1990 , vol. 31, # 9 p. 1245 - 1248
反应条件
1: boron trifluoride etherate / -78 °C
2: p-toluenesulphonic acid / benzene / Heating
View Scheme
参考文献
Pattenden, Gerald; Teague, Simon
Tetrahedron Letters, 1982 , vol. 23, # 13 p. 1403 - 1404
反应条件
1: 90 percent Turnov. / ZnCl2 / CH2Cl2 / 8 h / Ambient temperature
2: 66 percent / silicagel / CH2Cl2
View Scheme
参考文献
Reetz, Manfred T.; Heimbach, Horst
Chemische Berichte, 1983 , vol. 116, # 11 p. 3702 - 3707
