3,4-二甲基-3-戊烯-2-酮合成路线 (共 68 条)
反应条件
carbon disulfide; aluminium trichloride
参考文献
Krapiwin
Chem. Zentralbl., 1910 , vol. 81, # I p. 1336
反应条件
lithium salt of 2-nitropropane in N,N,N',N',N'',N''-hexamethylphosphoric triamide
5 h; Ambient temperatureIrradiation;
参考文献
Ono, Noboru; Tamura, Rui; Eto, Hiromichi; Hamamoto, Isami; Nakatsuka, Tamon; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3678 - 3684
反应条件
dihydrogen peroxide; methyltrioxorhenium (VII) in dichloromethane
48 h; Further byproducts given;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7728 - 7732
反应条件
aluminium trichloride in dichloromethane
参考文献
Hart,H.; Schlosberg,R.H.
Journal of the American Chemical Society, 1968 , vol. 90, # 19 p. 5189 - 5196
反应条件
tin(IV) chloride
T=0°C;
参考文献
Dubois, Jacques-Emile; Saumtally, Imran; Lion, Claude
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 3-4 p. 133 - 138
反应条件
alpha-methylbenzyl hydroperoxide; K12[ZnW(VO)2(ZnW9O34)2]*30H2O in 1,2-dichloro-ethane
T=20°C; 24 h;
参考文献
Adam, Waldemar; Alsters, Paul L.; Neumann, Ronny; Saha-Moeller, Chantu R.; Seebach, Dieter; Beck, Albert K.; Zhang, Rui
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8222 - 8231
反应条件
1: SnCl4
2: dimethylaniline
View Scheme
参考文献
Stevens
Journal of the American Chemical Society, 1934 , vol. 56, p. 451
Full Text Show Details
Colonge; Mostafavi
Bulletin de la Societe Chimique de France, 1939 , vol. <5>6, p. 344
反应条件
2,3-dimethyl aniline
参考文献
Stevens
Journal of the American Chemical Society, 1934 , vol. 56, p. 451
Full Text Show Details
Colonge; Mostafavi
Bulletin de la Societe Chimique de France, 1939 , vol. <5>6, p. 344
Full Text Show Details
Evans; Gillam
Journal of the Chemical Society, 1941 , p. 815,816
Full Text Show Details
Braude et al.
Journal of the Chemical Society, 1949 , p. 1890,1892
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Kocienski,P.J.; Ciabattoni,J.
Journal of Organic Chemistry, 1974 , vol. 39, # 3 p. 388 - 393
反应条件
tris(.mu.-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate; dihydrogen peroxide; sodium L-ascorbate in water; acetonitrile
T=0 - 2°C; optical yield given as percent dediastereoselective reaction;
参考文献
Kilic, Hamdullah; Adam, Waldemar; Alsters, Paul L.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1135 - 1140