2,7-二甲基辛-5-烯-4-酮合成路线 (共 4 条)
反应条件
bei der Ozonspaltung;
参考文献
Powell; Hagemann
Journal of the American Chemical Society, 1944 , vol. 66, p. 374
反应条件
trifluoroacetic acid in dichloromethane
Heating; Yield given;
参考文献
Ganapathi, Padma S.; Friedman, Simon H.; Kenyon, George L.; Rubin, Yves
Journal of Organic Chemistry, 1995 , vol. 60, # 10 p. 2954 - 2955
反应条件
1: 1.) LDA / 1.) THF, -78 deg C, 20 min, 2.) THF, from -78 deg C to 25 deg C
2: CF3COOH / CH2Cl2 / Heating
View Scheme
参考文献
Friedman; Ganapathi; Rubin; Kenyon
Journal of Medicinal Chemistry, 1998 , vol. 41, # 13 p. 2424 - 2429
反应条件
potassium hydroxide
Destillation des entstandenen Ketols in Gegenwart von Jod;
参考文献
Powell; Hagemann
Journal of the American Chemical Society, 1944 , vol. 66, p. 374