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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
68427-26-9
合成路线
（共 27 条）
159306-06-6
→
反应条件
6342-87-6
2,3-二氢-1H-苯并[e]茚-1-酮
+
68427-26-9
反应条件
cyclohexa-1,4-diene in chlorobenzene T=190°C; 8 h;
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
598-32-3
3-丁烯-2-醇
+
10151-46-9
萘-2-磺酰肼
→
反应条件
68427-26-9
反应条件
tetrabutylammomium bromide; oxygen; palladium diacetate in dimethyl sulfoxide; N,N-dimethyl-formamide T=70°C; Heck Reaction; P=760.051 Torr; Schlenk technique;
参考文献
Huang, Liangbin; Qi, Ji; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15462 - 15466
136240-69-2
→
反应条件
68427-26-9
反应条件
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide in dichloromethane 1 h; Molecular sieve 4A;
参考文献
ALLERGAN, INC.
Patent: US2006/111430 A1, 2006 ;
Location in patent: Page/Page column 26 ;
US 20060111430 A1
1449252-01-0
→
反应条件
68427-26-9
反应条件
4-(N,N-dimethlyamino)pyridine; acetic anhydride; triethylamine in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Watanabe, Eiichi; Kaiho, Atsushi; Kusama, Hiroyuki; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11744 - 11747
141-97-9
乙酰乙酸乙酯
+
939-26-4
2-(溴甲基)萘
→
反应条件
68427-26-9
反应条件
hydrogenchloride; sodium hydrogencarbonate; acetic acid in ethanol; water
参考文献
Eisai Co., Ltd.
Patent: US5719303 A1, 1998 ;
159305-89-2
→
反应条件
6342-87-6
2,3-二氢-1H-苯并[e]茚-1-酮
+
68427-26-9
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 5 h; Heating;
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
52762-83-1
+
78-94-4
丁烯酮
→
反应条件
68427-26-9
反应条件
palladium diacetate; silver(I) acetate; acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-Ichi; Ohe, Kouichi; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 8 p. 2341 - 2348
615-42-9
1,2-二碘苯
→
反应条件
68427-26-9
反应条件
1: 56 percent / Et3N, CuI / (Ph3P)2PdCl2 / tetrahydrofuran / Ambient temperature 2: 94 percent / Et3N, CuI / (Ph3P)2PdCl2 / tetrahydrofuran / Ambient temperature 3: 89 percent / PCC / CH2Cl2 / 8 h 4: 84 percent / diethyl ether / 0.5 h / Ambient temperature 5: 97 percent / K2CO3 / methanol / 0.5 h / Ambient temperature 6: 90 percent / PCC / CH2Cl2 / 2 h 7: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
37763-43-2
1-溴-2-(溴甲基)萘
→
反应条件
68427-26-9
反应条件
1: 67 percent / CaCO3, H2O / dioxane / 10 h / Heating 2: 97 percent / PCC / CH2Cl2 / 1 h 3: 95 percent / toluene / 4 h / Heating 4: 64 percent / H2 / 10percent Pd/C / ethyl acetate / 3 h / 1137.7 Torr 5: 52 percent / n-Bu3SnH, AIBN / benzene / 5 h / Heating View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
2586-62-1
1-溴-2-甲基萘
→
反应条件
68427-26-9
反应条件
1: 67 percent / NBS, benzoyl peroxide / CCl4 / 2 h / Heating 2: 67 percent / CaCO3, H2O / dioxane / 10 h / Heating 3: 97 percent / PCC / CH2Cl2 / 1 h 4: 95 percent / toluene / 4 h / Heating 5: 64 percent / H2 / 10percent Pd/C / ethyl acetate / 3 h / 1137.7 Torr 6: 52 percent / n-Bu3SnH, AIBN / benzene / 5 h / Heating View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
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