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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
68427-26-9
合成路线
（共 27 条）
3378-82-3
1-溴-2-萘甲醛
→
反应条件
68427-26-9
反应条件
1: 95 percent / toluene / 4 h / Heating 2: 64 percent / H2 / 10percent Pd/C / ethyl acetate / 3 h / 1137.7 Torr 3: 52 percent / n-Bu3SnH, AIBN / benzene / 5 h / Heating View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
76635-70-6
→
反应条件
68427-26-9
反应条件
1: 97 percent / PCC / CH2Cl2 / 1 h 2: 95 percent / toluene / 4 h / Heating 3: 64 percent / H2 / 10percent Pd/C / ethyl acetate / 3 h / 1137.7 Torr 4: 52 percent / n-Bu3SnH, AIBN / benzene / 5 h / Heating View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
150723-26-5
→
反应条件
68427-26-9
反应条件
1: 94 percent / Et3N, CuI / (Ph3P)2PdCl2 / tetrahydrofuran / Ambient temperature 2: 89 percent / PCC / CH2Cl2 / 8 h 3: 84 percent / diethyl ether / 0.5 h / Ambient temperature 4: 97 percent / K2CO3 / methanol / 0.5 h / Ambient temperature 5: 90 percent / PCC / CH2Cl2 / 2 h 6: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
159305-88-1
→
反应条件
68427-26-9
反应条件
1: 64 percent / H2 / 10percent Pd/C / ethyl acetate / 3 h / 1137.7 Torr 2: 52 percent / n-Bu3SnH, AIBN / benzene / 5 h / Heating View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
17450-63-4
→
反应条件
68427-26-9
反应条件
1: ethanol / Erwaermen des Reaktionsprodukts mit wss. NaOH 2: palladium/charcoal View Scheme
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
939-26-4
2-(溴甲基)萘
+
123-54-6
乙酰丙酮
→
反应条件
68427-26-9
反应条件
potassium carbonate in ethanol Heating;
参考文献
Goudie,A.C. et al.
Journal of Medicinal Chemistry, 1978 , vol. 21, # 12 p. 1260 - 1264
150723-27-6
→
反应条件
68427-26-9
反应条件
1: 89 percent / PCC / CH2Cl2 / 8 h 2: 84 percent / diethyl ether / 0.5 h / Ambient temperature 3: 97 percent / K2CO3 / methanol / 0.5 h / Ambient temperature 4: 90 percent / PCC / CH2Cl2 / 2 h 5: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
150723-28-7
→
反应条件
68427-26-9
反应条件
1: 84 percent / diethyl ether / 0.5 h / Ambient temperature 2: 97 percent / K2CO3 / methanol / 0.5 h / Ambient temperature 3: 90 percent / PCC / CH2Cl2 / 2 h 4: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
159306-05-5
→
反应条件
68427-26-9
反应条件
1: 90 percent / PCC / CH2Cl2 / 2 h 2: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
159306-03-3
→
反应条件
68427-26-9
反应条件
1: 97 percent / K2CO3 / methanol / 0.5 h / Ambient temperature 2: 90 percent / PCC / CH2Cl2 / 2 h 3: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
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