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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6846-13-5
合成路线
（共 21 条）
108-86-1
溴代苯
+
6846-13-5
→
反应条件
3328-86-7
+
2404-87-7
3-苯基噻吩
反应条件
P(O-biphenyl)(t-Bu)2; caesium carbonate; palladium diacetate in o-xylene 4 h; Heating; Product distribution; Further Variations:Reaction partnersReagentsSolvents;
参考文献
Journal of the American Chemical Society, , vol. 124, # 19 p. 5286 - 5287
6846-13-5
→
反应条件
34243-33-9
反应条件
1.1: trifluoromethanesulfonic anhydride; 2-chloropyridine / CH2Cl2 / -78 - 0 °C 1.2: 81 percent / CH2Cl2; tetrahydrofuran / -78 - 0 °C 2.1: 75 percent / ammonium hexafluorophosphate; 2-dicyclohexylphosphino-2',6'-dimethoxy-1,1'-biphenyl / CpRuCl(PPh3)2 / toluene / 105 °C View Scheme
参考文献
Movassaghi, Mohammad; Hill, Matthew D.
Journal of the American Chemical Society, 2006 , vol. 128, # 14 p. 4592 - 4593
108-86-1
溴代苯
+
6846-13-5
→
反应条件
3328-86-7
+
2404-87-7
3-苯基噻吩
反应条件
P(O-biphenyl)(t-Bu)2; caesium carbonate; palladium diacetate in o-xylene 4 h; Heating; Product distribution; Further Variations:Reaction partnersReagentsSolvents;
参考文献
Okazawa, Toru; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of the American Chemical Society, 2002 , vol. 124, # 19 p. 5286 - 5287
5813-89-8
2-噻吩甲酰胺
+
591-50-4
碘苯
→
反应条件
6846-13-5
反应条件
anhydrous iron chloride; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=135°C; 24 h; Inert atmosphere;
参考文献
Correa, Arkaitz; Elmore, Simon; Bolm, Carsten
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3527 - 3529
1003-31-2
2-氰基噻吩
+
591-50-4
碘苯
→
反应条件
6846-13-5
反应条件
copper(l) iodide; acetaldehyde oxime; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=120°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Dong-Xue; Xiang, Shi-Kai; Hu, Hao; Tan, Wen; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Tetrahedron, 2013 , vol. 69, # 47 p. 10022 - 10029
3437-95-4
2-碘噻吩
+
201230-82-2
+
74497-02-2
→
反应条件
6846-13-5
反应条件
potassium phosphate; Pd((imidazolium)acetonaphthene)(allyl)Cl in toluene T=90°C; P=760.051 Torr; 19 h; Schlenk technique;
参考文献
Fang, Weiwei; Deng, Qinyue; Xu, Mizhi; Tu, Tao
Organic Letters, 2013 , vol. 15, # 14 p. 3678 - 3681
3437-95-4
2-碘噻吩
+
74497-02-2
→
反应条件
6846-13-5
反应条件
sodium hydroxide; palladium diacetate in N,N-dimethyl-formamide T=60°C; P=760 Torr; 6 h;
参考文献
Bumagin, N. A.; Nikitin, K. V.; Beletskaya, I. P.
Doklady Chemistry, 1991 , vol. 320, # 4-6 p. 293 - 296
Dokl. Akad. Nauk SSSR Ser. Khim., 1991 , vol. 320, # 4 p. 887 - 890
1003-09-4
2-溴噻吩
+
103-71-9
异氰酸苯酯
→
反应条件
6846-13-5
反应条件
1: thien-2-yl bromide With manganese in tetrahydrofuran T=20°C; 2 h; 2: phenyl isocyanate in tetrahydrofuran T=20°C; 1 h;
参考文献
Rieke, Reuben D.; Suh, YoungSung; Kim, Seung-Hoi
Tetrahedron Letters, 2005 , vol. 46, # 35 p. 5961 - 5964
527-72-0
2-噻吩甲酸
+
701-73-5
苯基二硫代氨基甲酸甲酯
→
反应条件
6846-13-5
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide T=60°C; 0.05 h; Microwave irradiation;
参考文献
Kumar, Katari Naresh; Sreeramamurthy, Kintali; Palle, Sadananda; Mukkanti, Khagga; Das, Parthasarathi
Tetrahedron Letters, 2010 , vol. 51, # 6 p. 899 - 902
591-50-4
碘苯
+
29683-84-9
噻酚-2-甲醛肟
→
反应条件
6846-13-5
反应条件
CuSO4‵5H2O; potassium carbonate; N-methyl-2-(methylamino)ethylamine in o-xylene T=130°C; 12 h; regioselective reaction;
参考文献
Panda, Niranjan; Mothkuri, Raghavender; Nayak, Dinesh Kumar
European Journal of Organic Chemistry, 2014 , vol. 2014, # 8 p. 1602 - 1605
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