(3A'r,4'S,5'R,5A,8A'r,8B'r)-5'-甲氧基六氢二螺[环己烷-1,2'-[1,3]二氧杂环戊并[4,5-e][1,3]苯并二氧戊环-7',1''-环己烷]-4'-醇合成路线 （共 1 条）
6848-53-9(3A'r,4'S,5'R,5A,8A'r,8B'r)-5'-甲氧基六氢二螺[环己烷-1,2'-[1,3]二氧杂环戊并[4,5-e][1,3]苯并二氧戊环-7',1''-环己烷]-4'-醇
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反应条件
1: 94 percent / dimethylformamide / 12 h / 90 - 100 °C 2: 74 percent / tributyltin hydride, AIBN / toluene / 3 h / Heating 3: 83 percent / boron tribromide / CH2Cl2 / 5.5 h / Ambient temperature View Scheme
参考文献
Johnson; Dahl; Shih; Schedler; Anderson; Benjamin; Baker
Journal of Medicinal Chemistry, 1993 , vol. 36, # 23 p. 3628 - 3635
