4-乙酰基-4-甲基环己酮合成路线 （共 6 条）
反应条件
potassium hydroxide; water T=70°C; 6 h; Heating;
参考文献
Gray, George W.; Kelly, Stephen M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 26 - 31
反应条件
acetic anhydride
14 h; Heating;
参考文献
Gray, George W.; Kelly, Stephen M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 26 - 31
反应条件
1: H2O / Alkaline hydrolysis
2: acetic anhydride / 1 - 3 Torr
View Scheme
参考文献
Ahmed, M. Giasuddin; Ahmed, Syeda Asghari; Akhter, Kawsari; Tsuda, Yoshisuke; Hossain, M. Mahmun; Forsterling, F. Holger
Synthetic Communications, 2006 , vol. 36, # 9 p. 1273 - 1283
反应条件
sulfuric acid in ethanol
Heating;
参考文献
Inhoffen,H.H. et al.
Justus Liebigs Annalen der Chemie, 1966 , vol. 694, p. 19 - 30
反应条件
1: H2 / Raney-Ni / ethanol / 20 °C / 760 Torr
2: aq. H3PO4 / Heating
View Scheme
参考文献
Colonge,J. et al.
Bulletin de la Societe Chimique de France, 1966 , p. 1028 - 1031
反应条件
1: 93 percent / HCl / methanol
2: 90 percent / NH2-NH2, KOH / bis-(2-hydroxy-ethyl) ether
3: 78 percent / CH3COCl, SnCl4
4: 74 percent / CH2Cl2
View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Iyer, V. Sankar; Kok, Gaik B.
Magnetic Resonance in Chemistry, 1986 , vol. 24, p. 213 - 220
