4,5-双(苯甲酰硫基)-1,3-二硫杂环戊烯-2-硫酮合成路线 （共 25 条）
反应条件
sodium ethanolate in tetrahydrofuran; ethanol Heating;
参考文献
Meline, Ronald L.; Elsenbaumer, Ronald L.
Synthesis, 1997 , # 6 p. 617 - 619
反应条件
sodium ethanolate in tetrahydrofuran; ethanol Heating;
参考文献
Meline, Ronald L.; Elsenbaumer, Ronald L.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 16 p. 2467 - 2469
反应条件
NaOMe; aq. HCl in methanol (N2); MeOH soln. of NaOMe added to organic ligands in MeOH; mixt. stirred for 30 min; NiCl2*6H2O in MeOH added dropwise within 15 min; stirred for 1 h at room temp.; aq. HCl added; mixt. stirred in air overnight; washed with water and MeOH; dried in air; extracted with CS2; chromatographed on silica gel using CS2 as eluent; elem. anal.;
参考文献
Papavassiliou, George C.; Anyfantis, George C.; Steele, Barry R.; Terzis, Aris; Raptopoulou, Catherine P.; Tatakis, George; Chaidogiannos, George; Glezos, Nikos; Weng, Yufeng; Yoshino, Harukazu; Murata, Keizo
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2007 , vol. 62, # 5 p. 679 - 684
反应条件
sodium ethanolate Multistep reaction;
参考文献
Varma, K. Sukumar; Bury, Adrian; Harris, Nigel J.; Underhill, Allan E.
Synthesis, 1987 , # 9 p. 837 - 838
反应条件
sodium methylate 1.) MeOH, 30 min, 2.) MeOH, overnight; Yield given. Multistep reaction;
参考文献
Simonsen, Klaus B.; Svenstrup, Niels; Lau, Jesper; Simonsen, Ole; Mork, Pernille; Kristensen, Gitte J.; Becher, Jan
Synthesis, 1996 , # 3 p. 407 - 418
反应条件
sodium methylate 1.) MeOH, RT, 10 min, 2.) MeOH, RT, 3 h; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 6 p. 1773 - 1777
反应条件
sodium ethanolate 1.) EtOH, 2.) EtOH, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jorgensen, Tine; Girmay, Berhane; Hansen, Thomas K.; Becher, Jan; Underhill, Allan E.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 21 p. 2907 - 2912
反应条件
sodium 1.) EtOH, 2.) overnight; Yield given. Multistep reaction;
参考文献
Hansen, T. K.; Joergensen, T.; Jensen, F.; Thygesen, P. H.; Christiansen, K.; et al.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1359 - 1366
反应条件
1: 5,5'-(2-thioxo-1,3-dithide-4,5-diyl) bis(benzenecarbothiate) With sodium methylate in methanol T=20°C; 0.5 h; 2: 1-bromo-butane in methanol T=20°C; 2 h;
参考文献
Kimura, Shinya; Kurai, Hiroyuki; Mori, Takehiko; Mori, Hatsumi; Tanaka, Shoji
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 59 - 65
反应条件
in acetone
T=20°C; 4 h; Inert atmosphere;
参考文献
Shao, Min; Dongare, Prateek; Dawe, Louise N.; Thompson, David W.; Zhao, Yuming
Organic Letters, 2010 , vol. 12, # 13 p. 3050 - 3053
