4,5-双(苯甲酰硫基)-1,3-二硫杂环戊烯-2-硫酮合成路线 （共 25 条）
反应条件
in acetone
1.) r.t., 0.5 h, 2.) r.t., 2 h;
参考文献
Wang, Changsheng; Bryce, Martin R.; Batsanov, Andrei S.; Howard, Judith A. K.
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1679 - 1690
反应条件
in acetone
1.) r.t., 0.5 h, 2.) r.t., 2 h;
参考文献
Wang, Changsheng; Bryce, Martin R.; Batsanov, Andrei S.; Howard, Judith A. K.
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1679 - 1690
反应条件
in acetone
1.) r.t., 0.5 h, 2.) r.t., 2 h;
参考文献
Wang, Changsheng; Bryce, Martin R.; Batsanov, Andrei S.; Howard, Judith A. K.
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1679 - 1690
反应条件
1: carbon disulfide With tetraethylammonium phosphate
T=20°C; 0.0833333 h; Electrolysis;
2: mixed anhydride of acetic and benzoic acids T=20°C; 2 h; Electrolysis;
参考文献
Srivastav, Manish K.; Saraswat, Apoorv; Sharma, Laxmi Kant; Singh
Journal of the Indian Chemical Society, 2010 , vol. 87, # 9 p. 1131 - 1135
参考文献
Liu, Guoqun; Fang, Qi; Xu, Wen; Chen, Hongyu; Wang, Chunlei
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2004 , vol. 60, # 3 p. 541 - 550
反应条件
tetra-(n-butyl)ammonium iodide
1.) electrochemical reduction (Ag/AgCl-double-junction-electrode, -1.6 to -1.7 V), DMF, 48 h, 2.) room temp., 1 h; Yield given. Multistep reaction;
参考文献
Koster; Hartke
Archiv der Pharmazie, 1984 , vol. 317, # 12 p. 995 - 1002
参考文献
Saito, Gunzi; Hayashi, Hitoshi; Enoki, Toshiaki; Inokuchi, Hiroo
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 120, p. 341 - 344
反应条件
diiodomethane; sodium methylate in tetrahydrofuran
参考文献
Sony Corporation
Patent: US7425722 B2, 2008 ;
Location in patent: Page/Page column 12-14 ;
反应条件
sodium methylate
1.) THF, 45 min, 2.) 24 h; Yield given. Multistep reaction;
参考文献
Schulz, Reinhard; Schweig, Armin; Hartke, Klaus; Koester, Joachim
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4519 - 4528
反应条件
dicobalt octacarbonyl in benzene
3 h; Heating;
参考文献
Hansen, Thomas K.; Hawkins, Ian; Varma, K. Sukumar; Edge, Stephen; Larsen, Sine; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 1963 - 1966
