4,5-双(苯甲酰硫基)-1,3-二硫杂环戊烯-2-硫酮合成路线 （共 25 条）
反应条件
1: 5,5'-(2-thioxo-1,3-dithide-4,5-diyl) bis(benzenecarbothiate) With sodium methylate in methanol
T=20°C; 0.5 h;
2: ethyl bromide in methanol
T=20°C; 2 h;
参考文献
Kimura, Shinya; Kurai, Hiroyuki; Mori, Takehiko; Mori, Hatsumi; Tanaka, Shoji
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 59 - 65
反应条件
sodium methylate
1.) CH3OH, 20 min; Yield given. Multistep reaction;
参考文献
Schulz, Reinhard; Schweig, Armin; Hartke, Klaus; Koester, Joachim
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4519 - 4528
反应条件
1: 5,5'-(2-thioxo-1,3-dithide-4,5-diyl) bis(benzenecarbothiate) With sodium methylate in methanol
T=20°C; 0.5 h;
2: propyl bromide in methanol
T=20°C; 2 h;
参考文献
Kimura, Shinya; Kurai, Hiroyuki; Mori, Takehiko; Mori, Hatsumi; Tanaka, Shoji
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 59 - 65
反应条件
in benzene
T=60°C; 96 h;
参考文献
Saito, Katsuhiro; Ito, Kazuaki; Kabuto, Chizuko; Takahashi, Kensuke
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2383 - 2387
反应条件
72 h; Ambient temperature;
参考文献
Saito, Katsuhiro; Ito, Kazuaki; Kabuto, Chizuko; Takahashi, Kensuke
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2383 - 2387
