2-甲氧基-N-甲基苄胺合成路线 (共 12 条)
反应条件
1: With acetic acid in methanol; water T=20°C; 16 h; 2: With sodium tetrahydroborate in methanol; water T=0 - 20°C; 3 h;
参考文献
Molino, Bruce F.; Liu, Shuang; Guzzo, Peter R.; Beck, James P.
Patent: US2006/52378 A1, 2006 ;
Location in patent: Page/Page column 144 ;
US 20060052378 A1
反应条件
sodium tetrahydroborate in ethanol T=20°C; 20 h;
参考文献
Piazzi, Lorna; Belluti, Federica; Bisi, Alessandra; Gobbi, Silvia; Rizzo, Stefano; Bartolini, Manuela; Andrisano, Vincenza; Recanatini, Maurizio; Rampa, Angela
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 1 p. 575 - 585
反应条件
hydrogenchloride; sodium hydroxide in tetrahydrofuran
参考文献
US5672602 A1, ;
US 5672602 A
US5597845 A1, ;
反应条件
1: formic acid / 150 °C 2: aqueous hydrochloric acid View Scheme
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 280, p. 213,224
反应条件
1: LiAlH4 View Scheme
参考文献
Organic Letters, , vol. 1, # 11 p. 1851 - 1854
反应条件
sodium cyanoborohydride in methanol 72 h; Ambient temperature; Yield given;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 320, # 7 p. 647 - 654
反应条件
NaY faujasite T=90°C; 23 h;
参考文献
Tetrahedron Letters, , vol. 44, # 44 p. 8139 - 8142
反应条件
hexafluoroisopropyl alcohol T=20°C; 1 h;
参考文献
Chemical Communications, , vol. 50, # 15 p. 1836 - 1838
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 280, p. 213,224
反应条件
sodium tungstate; dihydrogen peroxide in methanol; water T=20°C;
参考文献
Colonna, Stefano; Pironti, Vincenza; Carrea, Giacomo; Pasta, Piero; Zambianchi, Francesca
Tetrahedron, 2004 , vol. 60, # 3 p. 569 - 575