in hexane stirred for 4 h at room temp. under Ar; ppt. (Ta-complex) was filtered off, soln. was passed through a SiO3 column (eluent THF), eluate evapd. to give PhCH=NBu-t;
参考文献
Journal of Organometallic Chemistry, , vol. 597, # 1-2 p. 61 - 68
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反应条件
in benzene-d6 heated at 165 ° C under Ar for 5 d; (1)H NMR monitoring; not isolated, yield given by NMR;
参考文献
Royo, Pascual; Sanchez-Nieves, Javier
Journal of Organometallic Chemistry, 2000 , vol. 597, # 1-2 p. 61 - 68
in hexane (Ar); addn. of oxaziridine to Cl2Ge(THF)Cr(CO)5; stirring for 4 h at room temperature; decantation; concn. of filtrate yielded PhCHN(t-Bu); drying of residue in vac. yielded (Cl2GeOCr(CO)5)(n);
参考文献
Journal of Organometallic Chemistry, , vol. 307, p. 205 - 218
Kokorev, G. I.; Litvinov, I. A.; Naumov, V. A.; Badrutdinov, Sh. Kh.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 8.2 p. 1852 - 1859,1655 - 1661
Kokorev, G. I.; Litvinov, I. A.; Naumov, V. A.; Badrutdinov, Sh. Kh.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 8.2 p. 1852 - 1859,1655 - 1661
Kokorev, G. I.; Litvinov, I. A.; Naumov, V. A.; Badrutdinov, Sh. Kh.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 8.2 p. 1852 - 1859,1655 - 1661
