6-甲氧基-2,3-二氢-1H-茚-1-甲腈合成路线 （共 7 条）
反应条件
chloro-trimethyl-silane; water; sodium iodide in acetonitrile
T=20°C; Reduction; 48 h;
参考文献
Kloubert, Stephane; Mathe-Allainmat, Monique; Andrieux, Jean; Langlois, Michel
Synthetic Communications, 2000 , vol. 30, # 16 p. 2873 - 2887
反应条件
Na2S2O5; trichlorophosphate
参考文献
Ray; Lahiri
Journal of the Indian Chemical Society, 1990 , vol. 67, # 4 p. 324 - 326
反应条件
1: 95 percent / ZnI2 / acetonitrile / 48 h / 20 °C
2: 77 percent / Me3SiCl; NaI; H2O / acetonitrile / 48 h / 20 °C
View Scheme
参考文献
Kloubert, Stephane; Mathe-Allainmat, Monique; Andrieux, Jean; Langlois, Michel
Synthetic Communications, 2000 , vol. 30, # 16 p. 2873 - 2887
反应条件
sodium tetrahydroborate in methanol
参考文献
Kloubert; Mathe-Allainmat; Andrieux; Sicsic; Langlois
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 23 p. 3325 - 3330
反应条件
1: SOCl2
2: NH3
3: 84 percent / POCl3, Na2S2O5
View Scheme
参考文献
Ray; Lahiri
Journal of the Indian Chemical Society, 1990 , vol. 67, # 4 p. 324 - 326
反应条件
1: NH3
2: 84 percent / POCl3, Na2S2O5
View Scheme
参考文献
Ray; Lahiri
Journal of the Indian Chemical Society, 1990 , vol. 67, # 4 p. 324 - 326
参考文献
H. Lundbeck A/S
Patent: US6352988 B2, 2002 ;
Location in patent: Page column 34 ;
US 6352988 B2
