3,5-双溴甲基-2,6-二甲基吡唑并[1,2-a]吡唑-1,7-二酮合成路线 (共 6 条)
反应条件
bromine in dichloromethane 0.5 h; Ambient temperatureother reaction time; chemical properties of 9,10-dioxabimanes: electrophylic reactions, reduction and oxidation, reactions with bases, thermal reactions; Product distribution;
参考文献
Kosower,E.M.; Pazhenchevsky,B.
Journal of the American Chemical Society, 1980 , vol. 102, p. 4983
反应条件
1: NH2NH2 / ethanol / 1 h / Heating 2: 73.1 percent / Cl2 / 1,2-dichloro-ethane / Heating 3: 12.5 percent / hydrated potassium carbonate / CH2Cl2 / 12 h / Ambient temperature 4: 2.2 percent / Br2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4983
反应条件
1: 12.5 percent / hydrated potassium carbonate / CH2Cl2 / 12 h / Ambient temperature 2: 2.2 percent / Br2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4983
反应条件
1: 73.1 percent / Cl2 / 1,2-dichloro-ethane / Heating 2: 12.5 percent / hydrated potassium carbonate / CH2Cl2 / 12 h / Ambient temperature 3: 2.2 percent / Br2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4983
反应条件
bromine in dichloromethane Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4983
反应条件
in acetonitrile 6 h; Ambient temperature;
参考文献
Kosower, Edward M.; Pazhenchevsky, Barak; Dodiuk, Hanna; Kanety, Hannah; Faust, Dov
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1666 - 1673