(2z)3-碘-2n-乙酰基巴豆酸甲酯合成路线 （共 4 条）
反应条件
1: With N-iodo-succinimide; trifluoroacetic acid in dichloromethane
T=20°C;
2: With triethylamine in dichloromethane
1 h;
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
反应条件
1.1: Et3N / methanol
2.1: NIS; TFA / CH2Cl2 / 20 °C
2.2: 40 percent / Et3N / CH2Cl2 / 1 h
View Scheme
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
反应条件
1.1: NaOAc
2.1: Et3N / methanol
3.1: NIS; TFA / CH2Cl2 / 20 °C
3.2: 40 percent / Et3N / CH2Cl2 / 1 h
View Scheme
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
反应条件
palladium diacetate; sodium carbonate in ethanol
T=55°C; Suzuki coupling; 4 h;
参考文献
Roff, Geoffrey J.; Lloyd, Richard C.; Turner, Nicholas J.
Journal of the American Chemical Society, 2004 , vol. 126, # 13 p. 4098 - 4099
