反应条件
1: 4-bromo-1-iodobenzene With iso-propylmagnesium bromide in tetrahydrofuran T=-40°C; 0.666667 h; Inert atmosphere; 2: With boric acid trimethyl ester in tetrahydrofuran T=-78 - 20°C; 38 h; Inert atmosphere; 3: 2,3-dimethylbutane-2,3-diol in toluene 10.5 h; RefluxInert atmosphere;
参考文献
Ito, Kazuta; Tamashima, Hiroto; Iwasawa, Nobuharu; Kusama, Hiroyuki
Journal of the American Chemical Society, 2011 , vol. 133, # 11 p. 3716 - 3719