反-1,2-二甲基环己胺合成路线 (共 74 条)
反应条件
methoxycarbonyl cyanide; sodium decatungstate in acetonitrile T=16°C; 22 h; Irradiation;
参考文献
Chemical Communications, , # 22 p. 2467 - 2468
反应条件
triethylsilane; triethyl aluminum sesquichloride in dichloromethane T=-15 - 20°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 126, # 33 p. 10319 - 10330
反应条件
hydrogen; AlPO2-Al2O3; platinum T=119.9°C; P=2475.2 Torr; further catalysts, hydrogen pressures, catalyst temperatures; Product distribution;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 91, # 9 p. 743 - 750
反应条件
tris(tetrabutylammonium)12-tungstophosphate in acetonitrile T=16°C; 22 h; Irradiation;
参考文献
Chemical Communications, , # 22 p. 2467 - 2468
反应条件
hydrogen; cationic chelate biphosphine rhodium in methanol T=20°C; P=760 Torr;
参考文献
Tetrahedron Letters, , vol. 25, # 13 p. 1393 - 1396
反应条件
hydrogen; cationic chelate biphosphine rhodium in dichloromethane T=20°C; P=760 Torr;
参考文献
Tetrahedron Letters, , vol. 25, # 13 p. 1393 - 1396
反应条件
osmium T=50 - 70°C; Hydrogenation;
参考文献
Chemische Berichte, , vol. 65, p. 1613,1617
Zhurnal Obshchei Khimii, , vol. 2, p. 755,760
反应条件
hydrogen; palladium on activated charcoal in 2,2,4-trimethylpentane T=25°C; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 115, # 5 p. 1934 - 1946
反应条件
hydrogenchloride; n-butyllithium; zirconocene dichloride 1.) from -78 deg C to 0 deg C; 2.) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 30, # 38 p. 5105 - 5108
反应条件
peracetic acid; cis-dichloro[N,N'-bis(2-pyridylmethyl)-1,2-ethanediamine]gallium(III) chloride in acetonitrile T=-0.16°C; Inert atmosphere;
参考文献
Inorganic Chemistry, , vol. 52, # 10 p. 5814 - 5823