反-1,2-二甲基环己胺合成路线 (共 74 条)
反应条件
peracetic acid in acetonitrile T=25°C; 0.166667 h; Product distribution; Further Variations:Reagents;
参考文献
Nehru, Kasi; Kim, Soo Jeong; Kim, In Young; Seo, Mi Sook; Kim, Youngmee; Kim, Sung-Jin; Kim, Jinheung; Nam, Wonwoo
Chemical Communications, 2007 , # 44 p. 4623 - 4625
反应条件
3-chloro-benzenecarboperoxoic acid; 5,10,15,20-tetrakis-pentafluorophenyl-21H,23H-porphyrin iron(III) chloride in dichloromethane; acetonitrile 1 h; Ambient temperatureother catalysts; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 4 p. 707 - 713
反应条件
methyl(trifluoromethyl)dioxirane in dichloromethane T=-22°C; 0.166667 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mello, Rossella; Fiorentino, Michele; Fusco, Caterina; Curci, Ruggero
Journal of the American Chemical Society, 1989 , vol. 111, # 17 p. 6749 - 6757
反应条件
peracetic acid; tris(.mu.-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate in acetonitrile T=30°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Lindsay Smith, John R.; Shul'pin, Georgiy B.
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4909 - 4912
反应条件
peracetic acid; tris(.mu.-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate in acetonitrile T=30°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Lindsay Smith, John R.; Shul'pin, Georgiy B.
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4909 - 4912
反应条件
peracetic acid; tris(.mu.-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate in acetonitrile T=30°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Lindsay Smith, John R.; Shul'pin, Georgiy B.
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4909 - 4912
反应条件
peracetic acid; tris(.mu.-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate in acetonitrile T=30°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Lindsay Smith, John R.; Shul'pin, Georgiy B.
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4909 - 4912
反应条件
C36H26FeN6O14; dihydrogen peroxide in water; acetonitrile T=20°C; 20 h; Irradiation;
参考文献
Cheng, Shi; Li, Jing; Yu, Xiaoxiao; Chen, Chuncheng; Ji, Hongwei; Ma, Wanhong; Zhao, Jincai
New Journal of Chemistry, 2013 , vol. 37, # 10 p. 3267 - 3273
反应条件
hydrogen; oxygen; acetic acid T=39.84°C; 0.166667 h; Large scale reaction;
参考文献
Yamanaka, Ichiro; Suzuki, Yuta; Toida, Masashi
Catalysis Today, 2010 , vol. 157, # 1-4 p. 286 - 290
反应条件
peracetic acid; Mn2O3(N,N',N''-trimethyl-1,4,7-triazacyclononane)2; dihydrogen peroxide in acetonitrile T=30°C; 1 h; reaction in the presence of m-CPBA as peroxy acid; oxidation of saturated hydrocarbons with "H2O2-manganese(IV)complex-peroxycarboxylic acid" reagent; selectivity; effect of peroxy acid; effect of reaction conditions, additives; Product distribution;
参考文献
Shul'pin; Lindsay-Smith
Russian Chemical Bulletin, 1998 , vol. 47, # 12 p. 2379 - 2386