triethyl borane in hexane; benzene addn. of hexane soln. of Et3B to a soln. of methyl cinnamate and Bu3SnH in benzene at 25°C under Ar, stirring for 15 h at 25°C; concn. in vac., chromy. on silica gel (hexane/ethyl acetate);
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 8 p. 2585 - 2587
in neat (no solvent) byproducts: H2; (N2), Schlenk techniques; sealing mixture of Bu3SnH and Ph3SnH under reduced pressure (5E-1 mm Hg), heating (200°C) for 5 h; NMR;
参考文献
Khan, Aman; Gossage, Robert A.; Foucher, Daniel A.
Canadian Journal of Chemistry, 2010 , vol. 88, # 10 p. 1046 - 1052
