in cyclohexane Irradiation (UV/VIS); under N2: irradiation of cyclohexane solns. of (C6H2(CH3)3Si(CH3)2)2 in presence of a 1-fold excess of (C4H9)3SnH and a 10-fold excess of CH3OSi(CH3)3 with an array of low-pressure mercury lamps at 254 nm for 4-12 h;; separation and purification by preparative gas chromatography;;
参考文献
Braddock-Wilking, Janet; Chaing, Michael Y.; Gaspar, Peter P.
Organometallics, 1993 , vol. 12, p. 197 - 209
Pereyre, M.; Valade, J.
Bulletin de la Societe Chimique de France, 1967 , p. 1928 - 1936
Full Text Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
in neat (no solvent) byproducts: H2; (N2), Schlenk techniques; sealing mixture of Bu3SnH and Ph3SnH under reduced pressure (5E-1 mm Hg), heating (200°C) for 5 h; NMR;
参考文献
Khan, Aman; Gossage, Robert A.; Foucher, Daniel A.
Canadian Journal of Chemistry, 2010 , vol. 88, # 10 p. 1046 - 1052
Pommier, J. C.; Valade, J.
Bulletin de la Societe Chimique de France, 1965 , p. 975 - 980
Full Text Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.7, page 69 - 97
Pommier, J. C.; Valade, J.
Bulletin de la Societe Chimique de France, 1965 , p. 975 - 980
Full Text Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.7, page 69 - 97
