in not given byproducts: C6H5C6H5COOC7H8O(CH2OCH3)O;
参考文献
Gandolfi et al.
Tetrahedron Letters, 1972 , p. 2063
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
Sawyer, A. K.; Brown, J. E.
Journal of Organometallic Chemistry, 1966 , vol. 5, p. 438 - 445
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.7, page 62 - 63
in 2,2,4-trimethylpentane Kinetics; Me3SiCH2 generated from Me3COOCMe3 and (Me3SiCH2)3As by laser flash photolysis; growth of Bu3Sn monitored at 400 or 450 nm;
参考文献
Wilt, James W.; Lusztyk, J.; Peeran, Mehoob; Ingold, K. U.
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 281 - 287
Davies, A. G.; Mitchell, T. N.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1896 - 1901
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
lithium aluminium tetrahydride; acetaldehyde; triethylamine in diethyl ether byproducts: ethanol; 1 equiv of diazoester adding to a mixt. of equimolar amts. of Ge deriv.and acetaldehyde at 0°C then treating with an excess of LiAlH4 in Et2O; analyzed by gas chromy. and NMR spectroscopy;
参考文献
Castel, A.; Riviere, P.; Satge, J.
Journal of Organometallic Chemistry, 1982 , vol. 232, # 2 p. 137 - 146
in neat (no solvent) byproducts: N2, ClCH2CO2CH2CH3; 1 equiv of diazoester adding slowly to an equimolar mixt. of Ge and Sn deriv. to result in exothermic reaction with N2 evolution; after 4 h at 20°C concg., diene ligand adding, heating in a sealed tube for 12h at 120°C; analyzed by gas chromy. and NMR spectroscopy;
参考文献
Castel, A.; Riviere, P.; Satge, J.
Journal of Organometallic Chemistry, 1982 , vol. 232, # 2 p. 137 - 146
