反应条件
triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran Sn-compd. addn. to stirred soln. of components and catalyst (room temp.,N2), stirring 2 h, quenching with satd. aq. KF, vigorous stirring overn ight, light petroleum addn., org. layer sepn., washing (water, brine), org. layer evapn. to dryness; residue chromy. (SiO2, Et2O/light petroleum 5:95), ratio E/Z>95:5;
参考文献
Boden, Christopher D. J.; Pattenden, Gerald; Ye, Tao
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 20 p. 2417 - 2419