Fischer, Jason M.; Piers, Warren E.; Pearce Batchilder, Susan D.; Zaworotko, Michael J.
Journal of the American Chemical Society, 1996 , vol. 118, # 1 p. 283 - 284
n-butyllithium; diisopropylamine in tetrahydrofuran
cooling of soln. of diisopropylamine in THF to -70°C for 10 min; addn. of n-BuLi for 5 min; after 15 min heating to room temp.; addn. of SnH(n-Bu)3 for 5 min; stirring at room temp. for 30 min; addn. of SiEt3Cl; stirring for 3 h at room temp.; evapn., chromy. on silica gel (hexanes);
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