1: (±)trans-2-azidocyclohexanol With triphenylphosphine in acetonitrile
T=80°C; 3 h;
2: p-toluenesulfonyl chloride With triethylamine in acetonitrile
T=-10 - 25°C;
参考文献
Lattanzi, Alessandra; Sala, Giorgio Della
European Journal of Organic Chemistry, 2009 , # 12 p. 1845 - 1848
Barton, Derek H. R.; Hay-Motherwell, Robyn S.; Motherwell, William B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 445 - 452
(CuOTf)2.C6H6; N-(2-pyridinylmethylene)-1-pentanamine in acetonitrile
72 h; various reagent ratios, dilutions; Product distribution;
参考文献
Albone, David P.; Aujla, Pavandeep S.; Taylor, Paul C.; Challenger, Stephen; Derrick, Andrew M.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9569 - 9571