反应条件
1: 35 percent / CH2Cl2; diethyl ether / undried Diazomethane solution; 1.) 0 deg C; 2.) room temp., 1 h 2: LiBH4 / 1,2-dimethoxy-ethane / 1.) -78 deg C; 2.) room temp., 2 h 3: Sodium methyl mercaptide, Tetraethylammonium chloride / H2O; CHCl3 / 4 h / Ambient temperature View Scheme
参考文献
Ottenheijm, Harry C.J.; Liskamp, Rob M.J.; Nispen, Simon P.J.M. van; Boots, Hans A.; Tijhuis, Marian W.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3273 - 3283
