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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
68890-32-4
合成路线
（共 6 条）
1357480-94-4
→
反应条件
68890-32-4
反应条件
copper diacetate; palladium diacetate; potassium carbonate in toluene 24 h; Inert atmosphereReflux;
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
69254-48-4
→
反应条件
68890-32-4
反应条件
copper diacetate; palladium diacetate; potassium carbonate in toluene 24 h; Inert atmosphereReflux;
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
1357480-93-3
→
反应条件
68890-32-4
反应条件
1: potassium carbonate / methanol; water / 2 h / 20 °C 2: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
39792-99-9
→
反应条件
68890-32-4
反应条件
1: bromine / acetic acid 2: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
13230-71-2
→
反应条件
68890-32-4
反应条件
1.1: iodine / dichloromethane / 15 h / 20 °C 2.1: potassium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 - 5 °C / Inert atmosphere 2.2: 17 h / 20 °C / Inert atmosphere; Reflux 3.1: potassium carbonate / methanol; water / 2 h / 20 °C 4.1: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
154138-43-9
→
反应条件
68890-32-4
反应条件
1.1: potassium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 - 5 °C / Inert atmosphere 1.2: 17 h / 20 °C / Inert atmosphere; Reflux 2.1: potassium carbonate / methanol; water / 2 h / 20 °C 3.1: copper diacetate; palladium diacetate; potassium carbonate / toluene / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Harada, Rika; Nishida, Naoto; Uchiito, Shiho; Onozaki, Yu; Kurono, Nobuhito; Senboku, Hisanori; Masao, Tokuda; Ohkuma, Takeshi; Orito, Kazuhiko
European Journal of Organic Chemistry, 2012 , # 2 p. 366 - 379
