1.1: tetrahydrofuran / 2 h / -78 °C 2.1: tetrafluoroboric acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 48 h / 20 °C 2.2: 48 h / 20 °C / 3800.26 Torr 3.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -78 °C 3.2: 16 h / 20 °C View Scheme
参考文献
Bagal, Sharan K.; Davies, Stephen G.; Fletcher, Ai M.; Lee, James A.; Roberts, Paul M.; Scott, Philip M.; Thomson, James E.
Tetrahedron Letters, 2011 , vol. 52, # 17 p. 2216 - 2220
hydrogen; tricarbonyl(.eta.(6)-1,2,3-trimethoxybenzene)chromium in tetrahydrofuran T=80°C; P=45600 Torr; 5 h; different catalysts, different temperatures;
参考文献
Maux, P. Le; Saillard, J.Y.; Grandjean, D.; Jaouen, G.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4524 - 4526
