1,1'-亚甲基二(3-甲基哌啶)合成路线 （共 4 条）
反应条件
1: With acetic anhydride; acetyl chloride in acetonitrile 1 h; Heating / reflux; 2: With sodium acetate in acetonitrile Heating / reflux; Product distribution / selectivity;
参考文献
YUHAN CORPORATION
Patent: WO2005/37823 A1, 2005 ;
Location in patent: Page/Page column 10 ;
反应条件
formaldehyd in acetaldehyde
参考文献
PETROLITE CORPORATION
Patent: EP383499 A3, 1990 ;
反应条件
in methanol
T=30°C; P=4500360 Torr; 120 h;
参考文献
Matsumoto, Kiyoshi; Hashimoto, Shiro; Ikemi, Yukio; Otani, Shinichi
Heterocycles, 1984 , vol. 22, # 6 p. 1417 - 1420
反应条件
in acetonitrile
20 h; Heating;
参考文献
Climent, Maria J.; Corma, Avelino; Dominguez, Irene; Iborra, Sara; Sabater, Maria J.; Sastre, German
Journal of Catalysis, 2007 , vol. 246, # 1 p. 136 - 146
