3-(1-甲氧基-1-甲基乙氧基)丙炔合成路线 （共 3 条）
反应条件
N.N'-bis[3,5-bis(trifluoromethyl)phenyl]thiourea
T=20°C; 20 h;
参考文献
Kotke, Mike; Schreiner, Peter R.
Synthesis, 2007 , # 5 p. 779 - 790
反应条件
1: 3-(2-methoxypropan-2-yloxy)prop-1-yne With ammonia; lithium; isoprene
T=-37°C; 1.5 h;
2: ethyl iodide 1.5 h;
参考文献
Bonrath, Werner; Pace, Francesco; Fischesser, Jocelyn; Witzgall, Konrad
Patent: US2012/197046 A1, 2012 ;
Location in patent: Page/Page column 7 ;
反应条件
1: 3-(2-methoxypropan-2-yloxy)prop-1-yne With piperylene; ammonia; lithium
T=-37°C; 1.5 h;
2: ethyl bromide 1.5 h; Product distribution / selectivity;
参考文献
Bonrath, Werner; Pace, Francesco; Fischesser, Jocelyn; Witzgall, Konrad
Patent: US2012/197046 A1, 2012 ;
Location in patent: Page/Page column 7 ;
