反应条件
1: 58 mg / m-chloroperbenzoic acid, 5percent sodium hydrogencarbonate / CH2Cl2 / 4 h / -15 °C
2: 77 mg / LAH / 1,2-dimethoxy-ethane; tetrahydrofuran / 2 h / Ambient temperature
3: 80 percent / lead(IV) acetate / pyridine / 0.5 h / Ambient temperature
4: 83 percent / diisobutylaluminium hydride (DIBAH) / 1,2-dimethoxy-ethane; hexane / 1.5 h / -78 - 0 °C
5: 84 percent / 4-(dimethylamino)pyridine, triethylamine / 16 h / Ambient temperature
View Scheme
参考文献
Murai, Akio; Ono, Mitsunori; Masamune, Tadashi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1202 - 1204