三丁基(2-甲基苯基)锡烷合成路线 （共 36 条）
反应条件
in dichloromethane 15 h; Ambient temperature;
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
aluminium trichloride in dichloromethane T=20°C; 15 h;
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); cesium fluoride in tetrahydrofuran T=50°C; Stille Cross Coupling; 6 h;
参考文献
Lee, Dong-Hwan; Qian, Yingjie; Park, Ji-Hoon; Lee, Jong-Suk; Shim, Sang-Eun; Jin, Myung-Jong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1729 - 1735
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride in 1,4-dioxane T=60°C; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 22 p. 6343 - 6348
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); cesium fluoride in tetrahydrofuran T=50°C; Stille Cross Coupling; 8 h;
参考文献
Lee, Dong-Hwan; Qian, Yingjie; Park, Ji-Hoon; Lee, Jong-Suk; Shim, Sang-Eun; Jin, Myung-Jong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1729 - 1735
反应条件
(tBuCN)2CuOTf; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate in ethyl acetate T=25°C; 12 h; Inert atmosphereGlovebox;
参考文献
Ye, Yingda; Sanford, Melanie S.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4648 - 4651
反应条件
1: CH2Cl2 / 15 h / Ambient temperature 2: H2O View Scheme
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
acrylic acid n-butyl ester; anhydrous lithium acetate; copper diacetate; palladium diacetate in N,N-dimethyl-formamide byproducts: butyl 3-(2-methylphenyl)propenoate; under Ar; 0.30-0.36 mmol of organotin comp. and 0.30 mmol of olefin added to a soln. of 0.03 mmol of Pd(OAc)2, 0.90 mmol of Cu(OAc)2 and 0.60 mmol of LiOAc in DMF at room temp., mixt. stirred at 100° for 24 h, diluted with Et2O; monitored by NMR spectra;
参考文献
Hirabayashi, Kazunori; Ando, Jun-Ichi; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 6 p. 1409 - 1417
反应条件
in tetrahydrofuran byproducts: o-tolylboronic acid; to srirred soln. of Sn-compound in THF was added soln. of BH3 in THF under N2, mixt. was left at room temp. for 1 h, refluxed for 1 h, cooled, Et2O and water was added; dried with MgSO4, solvent was removed under vac., column chromy. on silica gel with hexane and hexane-Et2O, recrystd. from water;
参考文献
Faraoni; Koll; Mandolesi; Zuniga; Podesta
Journal of Organometallic Chemistry, 2000 , vol. 613, # 2 p. 236 - 238
反应条件
borane; water in tetrahydrofuran 1 h; Heating;
参考文献
Faraoni; Koll; Mandolesi; Zuniga; Podesta
Journal of Organometallic Chemistry, 2000 , vol. 613, # 2 p. 236 - 238
